Strain-Controlled Low-Cycle Fatigue Behavior and Microstructure Evolution of the Hot-Work Die Steel at 700 °C.

Abstract

This study investigates the low-cycle fatigue behavior and microstructural evolution of a novel 30Cr2Ni3MoWV hot-work die steel at 700 °C under different strain amplitudes. High-temperature tensile tests demonstrated a tensile strength of 460 MPa and an elongation of 32%, confirming the material retains good ductility. Fracture analysis revealed ductile failure, supported by a 95% reduction in area. Low-cycle fatigue tests indicated notable cyclic softening at high strain amplitudes, with fatigue life declining rapidly as strain amplitude rose from 0.2% to 0.6%. A stress-softening coefficient model was established to describe this accelerated softening. Microstructural examination identified carbides (MC, M₇C₃, M₂₃C₆), which promoted secondary crack formation at 0.6% strain amplitude, contributing to early failure. TEM analysis further showed dislocation rearrangement, carbide coarsening, and martensite lath widening during cyclic loading. Among these, M₂₃C₆ precipitates were linked to increased softening at higher strains. The Coffin-Manson model parameters were optimized based on the relationship between fatigue life, plastic strain, and elastic strain. The model accurately predicted the steel's fatigue life, with only a 0.01% deviation from experimental results. This work correlates accelerated softening and reduced fatigue life with three microstructural mechanisms-carbide coarsening, dislocation accumulation, and secondary cracking-offering valuable guidance for enhancing the high-temperature performance of hot-work die steels.